PIHKALAnthologyShulgin_page_549

PIHKALAnthologyShulgin | page 549 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

dropwise over the course of 2 h. After a few min further stirring, the temperature was brought up to a gentle reflux on the steam bath, and then all was cooled again to 0 !C. The excess hydride was destroyed by the cautious addition of 18 mL IPA followed first by 5 mL of 15% NaOH and then by 15 mL…