PIHKALAnthologyShulgin_page_546

PIHKALAnthologyShulgin | page 546 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

h. The reaction mixture was then poured into H20, the layers separated, and the aqueous phase extracted with CH2C12. The extracts were pooled, washed with dilute aqueous KOH, and the solvents removed under vacuum. Distillation gave 0.7 g of 2,5-dimethoxyphenyl cyclopropyl sulfide with identical gas…