PIHKALAnthologyShulgin_page_543

PIHKALAnthologyShulgin | page 543 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

!C sharp. From IPA the product is a burnished gold color with the mp 106-107 !C. Anal. (C13HI7NOSS) C,H. A solution of LAH (40 mL ofa 1 M solution in THF) was cooled, under He, to 0 !C with an external ice bath. With good stirring there was added 1.05 mL 100% H2S04 dropwise, to minimize charring.…