PIHKALAnthologyShulgin_page_542

PIHKALAnthologyShulgin | page 542 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

46 2C-T-13; 2,5-DIMETHOXY-4-(2- METHOXYETHYLTHIO)PHENETHYLAMIN SYNTHESIS: To a solution of 3.25 g of KOH pellets in 25 mL hot MeOH, there was added 6.8 g of 2,5- dimethoxythiophenol (see under 2C-T-2 for its preparation) followed by 4.73 g of 2- methoxyethylchloride. This mixture was heated on the…