PIHKALAnthologyShulgin_page_540

PIHKALAnthologyShulgin | page 540 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

days, yielding a mixture of yellow crystals and a brown viscous syrup. The solids were separated and recrystallized from 40 mL MeOH to give 3.7 g 2,5-dimethoxy-4-(t)-butylthio-'-nitrostyrene as fine lemon- yellow crystals, with a mp of 93-94 !C. A second crop of 1.4 g had a mp of 91-92 !C. Anal.…