PIHKALAnthologyShulgin_page_539

PIHKALAnthologyShulgin | page 539 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

45 2C-T-9; 2,5-DIMETHOXY-4-(t)- BUTYLTHIOPHENETHYLAMINE SYNTHESIS: To a well-stirred ice-cold suspension of 2.8 g p-dimethoxybenzene and 3.2 mL N,N,NU,NU-tetramethylethylenediamine in 100 mL petroleum ether under an inert atmosphere of He, there was added 13 mL ofa 1.6 N solution of butyllithium in…