PIHKALAnthologyShulgin_page_536

PIHKALAnthologyShulgin | page 536 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

44 2C-T-8; 2,5-DIMETHOXY-4- CYCLOPROPYLMETHYLTHIOPHENETHYI SYNTHESIS: To a solution of 2.8 g of KOH pellets in 25 mL hot MeOH, there was added a mixture of 5.9 g 2,5-dimethoxythiophenol (see under 2C-T-2 for its preparation) and 5.0 g of cyclopropylmethyl bromide. There was an immediate exothermic…