PIHKALAnthologyShulgin_page_534

PIHKALAnthologyShulgin | page 534 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

2,5-dimethoxy-'-nitro-4-(n)-propylthiostyrene in 50 mL anhydrous THF. There was an immediate loss of color. After a few min further stirring, the tem-perature was brought up to a gentle reflux on the steam bath, then all was cooled again to 0 !C. The excess hydride was destroyed by the cautious…