PIHKALAnthologyShulgin_page_531

PIHKALAnthologyShulgin | page 531 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

MeOH, gave fine yellow crystals with a mp of 87.5-89 !C. Anal. (C19H23NO3S) C,H. A solution of 0.8 g 2,6-dimethoxy-4-(i-propylthio)benzaldehde in 10 mL nitromethane was treated with 0.2 g anhydrous ammonium acetate and heated on the steam bath for | h. The excess reagent/solvent was removed under…