PIHKALAnthologyShulgin_page_527

PIHKALAnthologyShulgin | page 527 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

2.72 g of a residue which was distilled at 140-145 !C at 0.2 mn/Hg to give 2.42 g ofa clear white oil. This was dissolved in 25 mL IPA, and neutralized with concentrated HCl. This gave a clear solution which, with good stirring, was diluted with 100 anhydrous Et2O to provide 2.40 g…