PIHKALAnthologyShulgin_page_510

PIHKALAnthologyShulgin | page 510 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

homologue remained an oil. Gas chromatographic analysis showed it to be about 90% pure, and it was used as obtained in the nitrostyrene steps with either nitromethane (here) or nitroethane (under DOPR). To a solution of 13 g 2,5-dimethoxy-4-(n)-propylbenzaldehyde in 100 mL nitromethane, there was…