PIHKALAnthologyShulgin_page_509

PIHKALAnthologyShulgin | page 509 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

36 2C-P; 2,5-DIMETHOXY-4-(n)- PROPYLPHENETHYLAMINE SYNTHESIS: To a stirred solution of 138 g p-dimethoxybenzene in 400 mL CH2C12 there was added a suspension of 172 g anhydrous AICI3 in 500 mL CH2C12 which contained 92.5 g propionyl chloride. After stirring for 1.5 h the reaction mixture was poured…