PIHKALAnthologyShulgin_page_506

PIHKALAnthologyShulgin | page 506 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

35 2C-O-4; 2,5-DIMETHOXY-4-(i)- PROPOXYPHENETHYLAMINE SYNTHESIS: To a solution of 3.10 g 85% KOH pellets in 30 mL warm MeOH there was added 6.16 g 2,5-dimethoxyphenol (there was immediate darkening) followed by 8.5 g isopropyl iodide. The reaction mixture was heated on the steam bath for 3.5 h.…