PIHKALAnthologyShulgin_page_504

PIHKALAnthologyShulgin | page 504 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

34 2C-N; 2,5-DIMETHOXY-4- NITROPHENETHYLAMINE SYNTHESIS: A cooled, stirred solution of 1.0 g 2,5-dimethoxyphenethylamine (see the recipe for 2C-H for its preparation) in 20 mL glacial acetic acid was treated with 3.3 mL 70% HNO3 in small portions, with the reaction temperature kept down with…