PIHKALAnthologyShulgin_page_487

PIHKALAnthologyShulgin | page 487 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

mp of 71-72 !C. The mother liquors on cautious treatment with H20, yielded, after EtOH recrystallization, | g additional product. Anal. (C12H1403) C,H. A solution of 150 mg aldehyde and an equal weight of malononitrile in 2.3 mL EtOH treated with 3 drops triethylamine gave immediate yellow crystals…