PIHKALAnthologyShulgin_page_482

PIHKALAnthologyShulgin | page 482 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

product that had a mp of 141-142 !C. Anal. (C11H1I5NO3) C,H,N. To a solution of 23.1 g flake KOH in 250 mL hot EtOH there was added 61.8 g 2,3-dimethyl-4- methoxyphenol followed by 60 g methyl iodide. This was held under reflux for 12 h, then stripped of solvent under vacuum. The residue was…