PIHKALAnthologyShulgin_page_481

PIHKALAnthologyShulgin | page 481 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

27 2C-G; 2,5-DIMETHOXY-3,4- DIMETHYLPHENETHYLAMINE SYNTHESIS: To a clear solution of 40.4 g flake KOH in 400 mL warm EtOH there was added 86.5 g 2,3-xylenol followed by 51.4 g methyl iodide. This mixture was held at reflux for 2 days, stripped of volatiles under vacuum, the residues dissolved in 1…