PIHKALAnthologyShulgin_page_480

PIHKALAnthologyShulgin | page 480 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

stripped of solvent, yielding a residual oil that was taken up in 10 mL of IPA, neutralized with concentrated HCl, and the generated solids diluted with anhydrous Et2O. The white crystalline 2,5- dimethoxy-4-fluorophenethylamine hydrochloride (2C-F) was recrystallized from IPA to give an air- dried…