PIHKALAnthologyShulgin_page_477

PIHKALAnthologyShulgin | page 477 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

with dilute NaOH, and extracted with 3x150 mL | N HCl. The pooled extracts were washed once with CH2C12 made basic with 25% NaOH, and extracted with 3x100 mL CH2C12. The combined organics were washed with saturated brine, and the solvent removed under vacuum to yield about 2 mL ofa colorless oil.…