PIHKALAnthologyShulgin_page_474

PIHKALAnthologyShulgin | page 474 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

approximately 15 mL of residue was dissolved in 300 mL CH2C12 and treated with 200 mL H20 containing 20 mL concentrated HCl. On shaking the mixture, there was deposited a mass of the hydrochloride salt which was diluted with a quantity of additional H20. The organic phase was extracted with…