PIHKALAnthologyShulgin_page_473

PIHKALAnthologyShulgin | page 473 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

course of 0.5 h. The stirred reaction mixture was allowed to come up to room temperature, then held on the steam bath for 1 h. The reaction mixture was poured into | L water, extracted with 3x75 mL CH2C12, and the pooled extracts washed with dilute HCl. The organic phase was stripped under vacuum…