PIHKALAnthologyShulgin_page_472

PIHKALAnthologyShulgin | page 472 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

24 2C-E; 2,5-DIMETHOXY-4- ETHYLPHENETHYLAMINE SYNTHESIS: A suspension of 140 g anhydrous AIC13 in 400 mL CH2Cl2 was treated with 100 g acetyl chloride. This slurry was added to a vigorously stirred solution of 110 g p-dimethoxybenzene in 300 mL CH2C12. Stirring was continued at ambient temperature…