PIHKALAnthologyShulgin_page_469

PIHKALAnthologyShulgin | page 469 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

g. These were recrystallized from 100 mL IPA providing yellow crystals of 2,5-dimethoxy-4-methyl-'- nitrostyrene which weighed, when dry, 7.70 g. The mp was 117-118 !C, and this was increased to 118- 119 !C upon recrystallization from benzene/heptane 1:2. To a well stirred suspension of 7.0 g LAH…