PIHKALAnthologyShulgin_page_468

PIHKALAnthologyShulgin | page 468 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

23 2C-D; LE-25; 2,5-DIMETHOXY-4- METHYLPHENETHYLAMINE SYNTHESIS: Into 1 L H20 that was being stirred magnetically, there was added, in sequence, 62 g toluhydroquinone, 160 mL 25% NaOH, and 126 g dimethyl sulfate. After about 2 h, the reaction mixture was no longer basic, and another 40 mL of the…