PIHKALAnthologyShulgin_page_462

PIHKALAnthologyShulgin | page 462 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

21 3C-BZ; 4-BENZYLOXY-3,5- DIMETHOXYAMPHETAMINE SYNTHESIS: A solution of 268 g 2,6-dimethoxyphenol and 212 g allyl bromide in 700 mL dry acetone was treated with 315 g anhydrous K2CO3 and held at reflux for 16 h. The solvent was removed under vacuum, and the residue dissolved in H2O and extracted…