PIHKALAnthologyShulgin_page_458

PIHKALAnthologyShulgin | page 458 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

20 2C-B; 4-BROMO-2,5- DIMETHOXYPHENETHYLAMINE SYNTHESIS: A solution of 100 g of 2,5-dimethoxybenzaldehyde in 220 g nitromethane was treated with 10 g anhydrous ammonium acetate, and heated on a steam bath for 2.5 h with occasional swirling. The deep-red reaction mixture was stripped of the excess…