
PIHKALAnthologyShulgin | page 455 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf
18 4-BR-3,5-DMA; 3,5-DIMETHOXY-4- BROMOAMPHETAMINE SYNTHESIS: The starting material 3,5-dimethoxy-4-bromobenzoic acid (made from the commercially available resorcinol by the action of methyl sulfate) was a white crystalline solid from aqueous EtOH with a mp of 248-250 !C. Reaction with thionyl…