PIHKALAnthologyShulgin_page_451

PIHKALAnthologyShulgin | page 451 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

16 BOHD; 2,5-DIMETHOXY-'-HYDROXY-4- METHYLPHENETHYLAMINE SYNTHESIS: A solution of 0.4 g 1-(2,5-dimethoxy-4-methylphenyl)- 1-methoxy-2-nitroethane (see preparation in the recipe for BOD) in 3.0 mL acetic acid was heated to 100 !C ona steam bath. There was added 1.0 g powdered zinc, followed by…