PIHKALAnthologyShulgin_page_449

PIHKALAnthologyShulgin | page 449 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

15 BOH; '-METHOXY-3,4- METHYLENEDIOXYPHENETHYLAMINE SYNTHESIS: To a solution of 30 g piperonal in 100 mL acetic acid there was added 20 mL nitromethane and 10 mL cyclohexylamine. After heating on the steam bath for 1.5 h, the reaction mixture started to crystallize. The mixture was cooled in an ice…