PIHKALAnthologyShulgin_page_446

PIHKALAnthologyShulgin | page 446 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

filtration and Et2O washed. When air-dried to constant weight, 4.49 g brilliant white crystals of 4-methyl- 2,5,'-trimethoxyphenethylamine hydrochloride (BOD) with a mp of 171-172 !C with decomposition, were obtained. The mother liquors on standing deposited 0.66 g additional crystals which were…