PIHKALAnthologyShulgin_page_441

PIHKALAnthologyShulgin | page 441 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

solution of butyllithium in hexane. After stirring for 10 min there was added 2.5 mL N-methylformanilide which led to an exothermic reaction. After another 10 min stirring, the reaction mixture was added to 100 mL dilute HCl, the phases were separated, and the aqueous phase extracted with 2x50 mL…