PIHKALAnthologyShulgin_page_432

PIHKALAnthologyShulgin | page 432 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

9 ASB; ASYMBESCALINE; 3,4-DIETHOXY-5- METHOXY PHENETHYLAMINE SYNTHESIS: To a solution of 32 g of 5-bromobourbonal in 150 mL DMF there was added 31 g ethyl iodide and 32 g of finely ground 85% KOH pellets. There was the formation ofa purple color and a heavy precipitate. On gradual heating to…