PIHKALAnthologyShulgin_page_422

PIHKALAnthologyShulgin | page 422 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

prior sintering at about 98 !C). This was recrystallized from 50 mL boiling 95% EtOH. After cooling in an ice bath, it was filtered, washed with EtOH, and air drying provided gold-yellow crystals with a mp of 105-106 !C. The proton NMR was excellent (in CDC13). A suspension of 2.0 g LAH in 100 mL…