PIHKALAnthologyShulgin_page_421

PIHKALAnthologyShulgin | page 421 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

6 ALEPH-6 2,5-DIMETHOXY-4- PHENYLTHIOAMPHETAMINE SYNTHESIS: To a 300 mL three-neck round-bottom flask set up with a magnetic stirrer and protected with a N2 atmosphere, there was added 75 mL hexane, 3.5 g tetramethylethylenediamine, and 4.2 g p- dimethoxybenzene. The reaction mixture was cooled to…